您好，欢迎访问山东省农业科学院文献资源数据库平台

Quantitative Analysis of 10 Mycotoxins in Wheat Flour by Ultrahigh Performance Liquid Chromatography-Tandem Mass Spectrometry with a Modified QuEChERS Strategy

文献类型： 外文期刊

作者： Zhou, Qingxin 1 ; Li, Fenghua 1 ; Chen, Leilei 1 ; Jiang, Dafeng 1 ;

作者机构： 1.Shandong Acad Agr Sci, Inst Agrofood Sci & Technol, Shandong Prov Key Lab Deep Proc Technol Agr Prod, Jinan 250100, Peoples R China

2.Shandong Ctr Dis Control & Prevent, Dept Chem & Phys, Shandong Ctr Food Safety Risk Assessment, Jinan 250014, Peoples R China

关键词： cereal products;mycotoxins;quantitative analysis;QuEChERS;UHPLC-MS/MS

期刊名称：JOURNAL OF FOOD SCIENCE （ 影响因子：3.167； 五年影响因子：3.376 ）

ISSN： 0022-1147

年卷期： 2016 年 81 卷 11 期

页码：

收录情况： SCI

摘要： A simple and sensitive analytical method for quantitative analysis of 10 mycotoxins was developed and validated by a combination of modified QuEChERS (quick, easy, cheap, effective, rugged, and safe) procedure with ultrahigh performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS). Sample preparation involved QuEChERS with dispersive solid phase extraction for clean-up, and analysis was performed by reversed-phase UHPLC-MS/MS using electrospray negative ionization and multiple reaction monitoring. Under optimized conditions, the calibration curves displayed good linear relationships with all coefficients of determinations (r(2)) higher than 0.998. The limits of quantification for all target mycotoxins were lower than 7 mu g/kg. Trueness and precision for the analytes were 70% to 116% average recoveries and 2% to 13% relative standard deviations (RSDs). The validated method was used to analyze 46 wheat flour samples for the targeted mycotoxins. The method can be used as a rapid and robust tool for screening mycotoxin in cereal products.

  • 相关文献

[1]Determination of 16 Mycotoxins in Maize by Ultrahigh-Performance Liquid Chromatography-Tandem Mass Spectrometry. Li, Xia,Liu, Bin,Wang, Fengen,Ma, Xinfeng,Li, Zengmei,Guo, Dongliang,Wang, Yutao,Deng, Ligang,Zhang, Shuqiu,Wan, Fachun. 2018

[2]Fast determination of multi-mycotoxins in corn by dispersive solid-phase extraction coupled with ultra-performance liquid chromatography with tandem quadrupole time-of-flight mass spectrometry. Wang Yan,Dong Yan-jie,Li Zeng-mei,Deng Li-gang,Guo Chang-ying,Zhang Shu-qiu,Zhao Shan-cang,Wang Yan,Li Da-peng. 2016

[3]Dissipation kinetics and residue of LH-2010A in cucumber and soil under greenhouse condition. Li, Ruijuan,Liu, Tongjin,Song, Guochun,Li, Rumei,Yu, Jianlei. 2015

[4]Determination and risk assessment of sixteen polycyclic aromatic hydrocarbons in vegetables. Li, Huidong,Lu, Xiao,Du, Hongxia,Guan, Shuai,Chen, Zilei,Li, Huidong,Zhu, Duanwei,Li, Huidong,Lu, Xiao,Du, Hongxia,Guan, Shuai,Chen, Zilei. 2018

[5]Analysis of 13 kinds of steroid hormones in raw milk using modified QuEChERS method combined with UPLC-QTOF-MS. Tan Xin-tong,Wang Ming-lin,Li Zeng-mei,Deng Li-gang,Zhao Shan-cang,Li Zeng-mei,Deng Li-gang,Zhao Shan-cang. 2016

[6]改良QuEChERS-气相色谱法测定韭菜中15种有机磷农药残留. 张仙,王小飞,彭西甜,胡西洲,刘军. 2017

[7]QuEChERS结合UPLC-MS/MS法测定番茄中吡蚜酮和吡丙醚残留量. 王小飞,张仙,彭茂民,夏虹. 2016

[8]QuEChERS—UPLC—MS/MS法同时测定羊奶中8种β-内酰胺类抗生素. 王帅帅,郑小平,孟瑾,何亚斌. 2015

[9]鲜牛乳及乳制品中4种雌激素含量的HPLC测定. 谭欣同,邓立刚,赵善仓,董燕婕,王燕,李增梅. 2015

[10]QuEChERS-超高效液相色谱-串联质谱法测定牛奶中6种头孢菌素类抗生素残留. 张小刚,王霞,戴春风,陈美莲. 2018

[11]QuEChERS-HPLC-MS/MS法检测液态乳中9种β_2-受体激动剂残留量. 李婧妍,郭春锋,崔立辉,刘拉平. 2016

[12]QuEChERS-高效液相色谱-串联质谱法测定水果中5种链格孢霉毒素. 陈跃,张悦丽,王超,常俊斌. 2019

[13]气相色谱-串联质谱法测定韭菜中拟除虫菊酯类农药残留. 张艳,陈子雷,郭长英,丁蕊艳,张文君,毛江胜,李慧冬. 2021

[14]超高效液相色谱-串联质谱法测定玉米中种菌唑残留. 梁京芸,苑学霞,董燕婕,范丽霞,赵善仓,王磊. 2020

[15]QuEChERS结合GC-MS/MS快速检测蔬菜中丁虫腈残留. 赵玉华,陈子雷,王玉涛,张树秋. 2016

[16]液相色谱-串联质谱在农药残留测定中的应用. 王晨晨,李慧冬,方丽萍,丁蕊艳,张文君,毛江胜,郭长英,陈子雷,杨国生. 2018

[17]QuEChERS-气相色谱-串联质谱法同时测定饲草中10种农药残留. 王峰恩,邓立刚,李霞,王文正,王磊,吕昆,张树秋. 2017

作者其他论文 更多>>
置顶
购物车
反馈

© 京ICP备09089781号-29 主办单位：山东省农业科学院文献资源数据库平台

学术资源： 中国农业科学院 农业专业知识服务系统 农科联盟资源共建共享平台 中国农业科技文献与信息服务平台 中国农业期刊集成服务平台