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A Survey of 61 Veterinary Drug Residues in Commercial Liquid Milk Products in China

文献类型： 外文期刊

作者： Shi, Runjia 1 ; Yu, Zhongna 2 ; Wu, Wei 1 ; Ho, Harvey 3 ; Wang, Jun 1 ; Wang, Yutao 4 ; Han, Rongwei 1 ;

作者机构： 1.Qingdao Agr Univ, Coll Food Sci & Engn, Qingdao 266109, Shandong, Peoples R China

2.Qingdao Agr Univ, Haidu Coll, Laiyang 265200, Shandong, Peoples R China

3.Univ Auckland, Auckland Bioengn Inst, Auckland, New Zealand

4.Shandong Acad Agr Sci, Inst Qual Stand & Test Technol Agroprod, Jinan 250100, Peoples R China

关键词： Charm rapid test kit; China; Liquid milk; Ultraperformance liquid chromatography-tandem mass spectrometry; Veterinary drug residues

期刊名称：JOURNAL OF FOOD PROTECTION （ 影响因子：2.077； 五年影响因子：2.224 ）

ISSN： 0362-028X

年卷期： 2020 年 83 卷 7 期

页码：

收录情况： SCI

摘要： To investigate the drag residue status in commercial liquid milk products in China, 190 samples, including ultrahigh temperature milk (n = 168) and pasteurized milk (n = 22) samples, were collected in 2019. Milk samples were analyzed for the presence of any of the 61 veterinary drugs in them by using a screening assay combined with an ultraperformance liquid chromatography-tandem mass spectrometry analysis. Ten (5.26%) samples were found positive for beta-lactams, tetracyclines, and aminoglycosides, and six (3.16%) samples were confirmed residual for penicillin G (n = 6; 3.16%), tetracycline (n = 1; 0.53%), and oxytetracycline (n = 1; 0.53%), with the maximum concentration of 2.85, 40.64, and 12.35 mu g kg(-1), respectively. Drag residue detection rate in group II (4.55%; the local city domestic brands) was higher than that in group I (2.70%; the major brands of China) and group III (2.78%; the imported brands into China) and higher in domestic samples (3.39%) than that in imported samples (2.78%), and higher in pasteurized milk samples (9.09%) than in ultrahigh temperature milk samples (2.38%). All drag residue levels were far below the regulated maximum residue limits. However, based on some veterinary drag residues detected in the samples, there is a potential veterinary drug risk in liquid milk products in the Chinese market, and this situation deserves the attention of governments and consumers.

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