EXTRACTION AND ISOLATION OF DICTAMNINE, OBACUNONE AND FRAXINELLONE FROM Dictamnus dasycarpus TURCZ. BY SUPERCRITICAL FLUID EXTRACTION AND HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY
文献类型： 外文期刊
作者： Wang, Daijie 1 ; Lin, Yunliang 1 ; Lin, Xiaojing 1 ; Geng, Yanling 1 ; Wang, Xiao 1 ; Zhang, Jinjie 2 ; Qiu, Jiying 3 ;
作者机构： 1.Shandong Acad Sci, Proc Control Res Ctr TCM, Shandong Anal & Test Ctr, Jinan 250014, Peoples R China
2.Zhejiang Univ, Coll Biosyst Engn & Food Sci, Hangzhou 310030, Zhejiang, Peoples R China
3.Shandong Acad Agr Sci, Inst Agrofood Sci & Technol, Jinan 250100, Shandong, Peoples R China
关键词： Dictamnus dasycarpus; dictamnine; obacunone
期刊名称：QUIMICA NOVA （ 影响因子：0.961； 五年影响因子：1.091 ）
ISSN： 0100-4042
年卷期： 2012 年 35 卷 2 期
页码：
收录情况： SCI
摘要： Supercritical fluid extraction was used to extract active compounds from the Chinese traditional medicinal D. dasycarpus under the pressure of 30 MPa and temperature of 45 degrees C. Further separation and purification was established by high-speed counter-current chromatography (HSCCC) with a two-phase solvent system composed of n-hexane-ethyl acetate-methanol-water (1:0.8:1.3:0.9, volume ratio). The separation yielded a total of 47 mg of dictamnine, 24 mg of obacunone and 83 mg of fraxinellone from 1.0 g of the crude extract in one step separation with the purity of 99.2, 98.4 and 99.0%, respectively, as determined by HPLC. The chemical structures of these compounds were identified by ES1-MS, IR, H-1-NMR and C-13-NMR.
- 相关文献
作者其他论文 更多>>
-
Biodegradable PBAT microplastics adversely affect pakchoi (Brassica chinensis L.) growth and the rhizosphere ecology: Focusing on rhizosphere microbial community composition, element metabolic potential, and root exudates
作者：Han, Yujuan;Wang, Xiao;Wen, Dan;Yan, Dong;Yang, Ning;Teng, Ying;Gao, Peixin;Yang, Ning
关键词：PBAT microplastics; Plant growth; Rhizosphere microbiome; Root exudates
-
Formulation of the microbial agent Bacillus amyloliquefaciens NCPSJ7 and its application against Botrytis cinerea in tomato
作者：Wang, Junhua;Zhang, Xingwang;Zhang, Yanhao;Qin, Shunxin;Qiu, Jiying;Zhang, Ziyue;Chen, Xiangyan;Chen, Leilei;Zhou, Qingxin;Qin, Shunxin;Zhou, Qingxin;Li, Xihong;Zhou, Qingxin
关键词：Bacillus amyloliquefaciens; Spray drying; Botrytis cinerea; Tomatoes; Microbial agent; Biopesticides
-
MicroRNA sequence variation can impact interactions with target mRNA in cattle
作者：Hao, Dan;Thomsen, Bo;Holm, Lars-Erik;Hao, Dan;Yang, Yu;Chen, Hong;Wang, Xiao;Wang, Xiao
关键词：Cattle; MicroRNA; Single -nucleotide polymorphism; Quantitative trait locus
-
Lactate and Lactylation: Clinical Applications of Routine Carbon Source and Novel Modification in Human Diseases
作者：Wang, Zhimin;Zhao, Shuiying;Hao, Dan;Hao, Dan;Zhang, Ziyin;Zeng, Zhen;Wang, Xiao;Wang, Xiao
关键词：
-
Harnessing male germline epigenomics for the genetic improvement in cattle
作者：Wang, Xiao;Li, Wenlong;Feng, Xia;Yu, Ying;Wang, Xiao;Wang, Xiao;Li, Jianbing;Liu, George E.;Fang, Lingzhao
关键词：Artificial insemination; Cattle; Epigenetic inheritance; Genetic improvement; Germline epigenomics
-
Identification of target genes and pathways related to heat tolerance in Chinese Holstein cows
作者：Li, Rongling;Ahmad, Muhammad Jamil;Yang, Liguo;Li, Rongling;Hou, Minghai;Wang, Xiao;Li, Jianbin;Jiang, Qiang;Huang, Jinming;Liu, Shenhe
关键词：Dairy cows; Heat stress; miRNAs; RNA sequencing; Temperature-humidity index
-
The single-cell transcriptome and chromatin accessibility datasets of peripheral blood mononuclear cells in Chinese holstein cattle
作者：Wang, Xiao;Zhang, Fan;Wang, Kun;Zhang, Miao;Li, Rongling;Gao, Yundong;Li, Jianbin;Gao, Yahui;Li, Cong-jun;Liu, George E.;Fang, Lingzhao;Zhao, Xiuxin;Zhang, Yuanpei;Cai, Gaozhan;Xue, Guanghui;Liu, Yan;Wang, Lingling
关键词：Chinese Holstein cattle; Peripheral blood mononuclear cell; Lipopolysaccharide; Single-cell accessibility dataset; Transcriptome; Chromatin
