文献类型: 外文期刊
作者: Deng, Ligang 1 ; Chen, Lu 1 ; Guan, Shuai 1 ; Liu, Junhua 1 ; Liang, Jingyun 1 ; Li, Xia 1 ; Li, Zengmei 1 ;
作者机构: 1.Shandong Acad Agr Sci, Inst Agr Qual Stand & Testing Technol Res, Key Lab Test Technol Food Qual & Safety Shandong, 202 Gongyebeilu Rd, Jinan 250100, Peoples R China
关键词: emamectin benzoate; rice; residue; degradation; UPLC-MS/MS
期刊名称:MOLECULES ( 影响因子:4.411; 五年影响因子:4.587 )
ISSN:
年卷期: 2020 年 25 卷 3 期
页码:
收录情况: SCI
摘要: The experiment developed the ultra-high-performance liquid chromatography-tandem mass spectrometry (UPLC/MS/MS) method for testing emamectin benzoate, and studied the metabolism of emamectin benzoate in rice plants and rice-growing environments via application of this testing method. The dissipation curve of emamectin benzoate standard substance was good at 0.5-200 mu g L-1, and its correlation coefficient was greater than 0.99. In the concentration range of 0.1-50 mu g kg(-1), the average recovery rate of plants, soil, and field water was 82 %-102 %, and relative standard deviation (RSD) was between 0.3 % and 15.9 %. Half-lives in rice plants and soil were 0.8-2.8 days and 1.9-3.8 days, respectively, and emamectin benzoate was not detected in rice or rice hull. The experiment showed that emamectin benzoate is harmless to human health at the concentration recommended by the manufacturer.
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